凝胶注模成型刚玉-尖晶石多孔陶瓷的制备

Preparation of Alumina-spinel Porous Ceramics by Gelcasting

  • 摘要: 为拓展凝胶注模成型工艺在多孔陶瓷制备中的应用,用粘度计对刚玉-尖晶石复合浆料的流变学特性进行研究,并采用萘、淀粉、聚乙烯醇作为造孔剂,用凝胶注模成型方法制备出一系列刚玉-尖晶石多孔陶瓷.经过排胶、烧结等步骤,并对成型坯体进行X-射线衍射法测定气孔率,最高气孔率为52.8%,体积密度为1.84 g.cm-3,说明凝胶注模成型是制备多孔陶瓷的有效方法.

     

    Abstract: In order to widen the application of gelcasting in porous ceramics,rheological behavior of alumina-spinel(3∶1) slurries is studied using viscometry.Naphtalene,fecula and polyvinyl alcohol were used as pore-forming additives.A series of alumina-spinel(3∶1) porous ceramics were prepared by gelcasting.After burning out sintering and measuring the porosity applying X-ray diffraction,the hightest level of porosity is found to be 52.8% and the volume density(1.84 g·cm-3.) It is shown that the method is effective for the preparation of porous ceramics.

     

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